Caprock Integrity Assessment from Core-Based Formation Analysis and Laboratory Workflow: A Case Study of The Asri Basin Caprock
DOI:
https://doi.org/10.29017/scog.v49i1.2021Keywords:
Caprock integrity, core analysis, formation stratigraphy, petrophysics, rock mechanismAbstract
Caprock integrity is a critical factor in ensuring the long-term safety of CO₂ geological storage, enhanced oil recovery (EOR), and wellbore stability. This study investigates the sealing performance of shale- and carbonate-rich caprock intervals from the Asri Basin, with specific focus on the Baturaja and Gita Formations. This study introduces a CT-guided integrated laboratory workflow for caprock integrity assessment, which simultaneously links petrophysical sealing capacity, mineralogical controls, and geomechanical strength within a unified experimental framework, a workflow rarely applied in Southeast Asian basins. Whole-core sections from Well ASR-1 were screened using computed tomography (CT) imaging to identify fractures and heterogeneity prior to plug extraction. Laboratory methods included porosity and permeability determination under variable confining stresses, mercury injection capillary pressure (MICP) analysis to evaluate sealing capacity, mineralogical characterization by X-ray diffraction (XRD), scanning electron microscopy (SEM–EDS), petrography, and mechanical testing (UCS, triaxial, and Brazilian tensile tests). The results demonstrate significant depth-dependent variability: The Baturaja Formation exhibited heterogeneous sealing capacity, with entry pressures ranging from 217 to 1,197 psi, while the Gita Formation consistently displayed strong sealing, with maximum Pc_entry of 2,844 psi and pore systems dominated by <0.1 µm throats. Mechanical tests confirmed adequate strength and the preservation of low permeability under confining stress, with clay content and carbonate cementation identified as primary controls on integrity. The integrated workflow enables a process-based interpretation of lithology-controlled sealing mechanisms, improving the robustness of site selection and risk assessment for CO₂ storage in the Asri Basin and similar carbonate and mudstone systems.
References
Ajayi, T., J. S. Gomes, and A. Bera. 2019. “A Review of CO2 Storage in Geological Formations Emphasizing Modeling, Monitoring and Safety.” Petroleum Science and Technology. doi:10.1007/s12182-019-0340-8.
Ali, M. 2021. “Influence of Pressure, Temperature and Organic Surface Concentration on Hydrogen Wettability of Caprock; Implications for Hydrogen Geo-Storage.” Energy Reports 7:5988–96. doi:10.1016/j.egyr.2021.09.016.
Al-Yaseri, Ahmed, Abduljamiu Amao, and Ahmed Fatah. 2023. “Experimental Investigation of Shale/Hydrogen Geochemical Interactions.” Fuel 346:128272. doi:10.1016/j.fuel.2023.128272.
Ao, Xiang, Yiyu Lu, Jiren Tang, Yuting Chen, and Honglian Li. 2017. “Investigation on the Physics Structure and Chemical Properties of the Shale Treated by Supercritical CO 2.” Journal of CO2 Utilization 20:274–81. doi:10.1016/j.jcou.2017.05.028.
Bera, A., B. Shukla, and D. Jogani. 2025. “A Perspective Review of Applications of the Computed Tomography (CT) Scan Imaging Technique for Microscopic Reservoir Rock Characterization.” Deep Underground Science and Engineering. doi:10.1002/dug2.12138.
Boulin, P. F., P. Bretonnier, and V. Vassil. 2013. “Seal Capacity: Influence of Stress and Geometry on Capillary Entry Pressure.” Marine and Petroleum Geology 48:64–73. doi:10.1016/j.marpetgeo.2013.07.010.
Bourbiaux, B. 2007. “Multi-Scale Characterization of an Heterogeneous Aquifer Through the Integration of Geological, Geophysical and Flow Data: A Case Study.” Oil & Gas Science and Technology 62(3):347–73. doi:10.2516/ogst.
Busch, A., S. Alles, Y. Gensterblum, D. Prinz, D. N. Dewhurst, M. D. Raven, H. Stanjek, and B. M. Krooss. 2008. “Carbon Dioxide Storage Potential of Shales.” International Journal of Greenhouse Gas Control 2(3):297–308. doi:10.1016/j.ijggc.2008.03.003.
Chiquet, P., J. L. Daridon, D. Broseta, and S. Thibeau. 2007. “Wettability Alteration of Caprock Minerals by Carbon Dioxide.” Geofluids 7(2):112–22. doi:10.1111/j.1468-8123.2007.00168.x.
Choi, C. S., J. Kim, and J. J. Song. 2021. “Analysis of Shale Property Changes after Geochemical Interaction under CO2 Sequestration Conditions.” Energy 214:118933. doi:10.1016/j.energy.2020.118933.
Destiana, Syifa, Dedy Irawan, Prasandi Abdul Aziz, and Ika Merdekawati. 2025. “CO2 Storage Screening Criteria Based on Seal Capacity in Indonesia.” Scientific Contributions Oil and Gas 48(4). https://doi.org/10.29017/scog.v48i4.1829
Farokhpoor, R., B. J. A. Bjørkvik, E. Lindeberg, and O. Torsæter. 2013. “Wettability Behaviour of CO2 at Storage Conditions.” International Journal of Greenhouse Gas Control 12:18–25. doi:10.1016/j.ijggc.2012.11.003.
Fisher, Q. J., M. Casey, S. D. Harris, and R. J. Knipe. 2001. “Uncertainty in Fault Seal Parameters: Implications for Hydrocarbon Retention.” Marine and Petroleum Geology 18(4):469–88. doi:10.1016/S0264-8172(00)00064-7.
Hansen, O. R. 2020. “Caprock Integrity Assessment from MICP, Pore Pressure and Geomechanical Constraints.” Marine and Petroleum Geology 121:104603. doi:10.1016/j.marpetgeo.2020.104603.
Kadyrov, R., E. Statsenko, and T. H. Nguyen. 2024. “Integrating ΜCT Imaging of Core Plugs and Transfer Learning for Automated Reservoir Rock Characterization and Tomofacies Identification.” Marine and Petroleum Geology 165:107014. doi:10.1016/j.marpetgeo.2024.107014.
Klewiah, I., D. S. Berawala, H. C. A. Walker, P. Ø. Andersen, and P. H. Nadeau. 2020. “Review of Experimental Sorption Studies of CO2 and CH4 in Shales.” Journal of Natural Gas Science and Engineering 74:103045. doi:10.1016/j.jngse.2019.103045.
Liang, Z. 2022. “Study and Classification of Porosity Stress Sensitivity in Shale.” ACS Omega 7(31):27377–90. doi:10.1021/acsomega.2c03393.
Lin, R. 2022. “Stress and Pressure Dependent Permeability of Shale Rock: Discrete Element Method (DEM) Simulation on Digital Core.” Journal of Petroleum Science and Engineering 208:109797. doi:10.1016/j.petrol.2021.109797.
Lohr, C. D., and P. C. Hackley. 2018. “Using Mercury Injection Pressure Analyses to Estimate Sealing Capacity of the Tuscaloosa Marine Shale in Mississippi, USA: Implications for Carbon Dioxide Sequestration.” International Journal of Greenhouse Gas Control 75:186–99. doi:10.1016/j.ijggc.2018.09.006.
Miocic, J. M., G. Johnson, and C. E. Bond. 2019. “Uncertainty in Fault Seal Parameters: Implications for CO2 Column Height Retention and Storage Capacity in Geological CO2 Storage Projects.” Solid Earth 10(3):951–67. doi:10.5194/se-10-951-2019.
Mouzakis, Katherine M., Alexis K. Navarre-Sitchler, Gernot Rother, José Leobardo Bañuelos, Xiuyu Wang, John P. Kaszuba, Jason E. Heath, Quin R. S. Miller, Vladimir Alvarado, and John E. McCray. 2016. “Experimental Study of Porosity Changes in Shale Caprocks Exposed to CO2-Saturated Brines I: Evolution of Mineralogy, Pore Connectivity, Pore Size Distribution, and Surface Area.” Environmental Engineering Science 33(10):725–35. doi:10.1089/ees.2015.0588.
Nugraha, Fanata Y., M. Firdaus Al Hakim, Brian Tony, Damar Nandiwardhana, and Steven Chandra. 2024. “Development of CO2 Hub-Clustering Management in The South Sumatra Basin.” Scientific Contributions Oil and Gas 47(1). https://doi.org/10.29017/SCOG.47.1.1607
Olabode, A., and M. Radonjic. 2014. “Characterization of Shale Cap-Rock Nano-Pores in Geologic CO2 Containment.” Environmental & Engineering Geoscience 20(4):361–70. doi:10.2113/gseegeosci.20.4.361.
Paulsen, S. 2022. “Quantifying Caprock Integrity under CO2 Injection: Integrating Geomechanics and Petrophysics.” Marine and Petroleum Geology 143:105588. doi:10.1016/j.marpetgeo.2022.105588.
Purba, Humbang, Bagus D. Prasetyo, Ricky Andrian Tampubolon, Pradityo Riyadi, Shidqi Anugrah Diria, and Argya H. Basundara. 2017. “Pemisahan Litologi Dan Fluida Dengan Menggunakan Poisson Impedance (Distinguishing Lithology and Fluid Using Poisson Impedance).” Lembaran Publikasi Minyak Dan Gas Bumi 51(3). https://doi.org/10.29017/LPMGB.51.3.25
Skerbisch, A. 2025. “Caprock Integrity Assessment for CO2 Storage: Core-Scale Workflow Integrating XRD, SEM-EDS, CT and MICP.” International Journal of Greenhouse Gas Control 138:104434. doi:10.1016/j.ijggc.2025.104434.
Zou, Y. 2018. “Effects of CO2–Brine–Rock Interaction on Porosity/Permeability and Mechanical Properties during Supercritical-CO2 Fracturing in Shale Reservoirs.” Journal of Natural Gas Science and Engineering 53:102–15. doi:10.1016/j.jngse.2017.11.004.
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